Dennis Nicks' Research Experience:

The Diffusion Denuder/Sulfur Chemiluminescence Detector (DD/SCD) and the Continuous Sulfur Dioxide Detector (CSD) for ultra-trace measurement of sulfur dioxide in air.
Since 1993, I have been developing instrumentation for measuring ultra-trave levels of sulfur dioxide in the atmosphere. I was a co-developer of the Diffusion Denuder/Sulfur Chemiluminescence Detector (DD/SCD). The DD/SCD has a detection limit of < 20 parts-per-trillion by volume (pptv) for a 10 minute measurement. The DD/SCD has been validated as a sensitive, interference-free technique in an experiment sponsored by the National Science Foundation (NSF).

Currently, a new version of the DD/SCD called the Continuous Sulfur Dioxide Detector (CSD) is being developed by myself and my advisor, Dr. Richard Benner. The CSD benefits from a redesigned denuder manifold and optimized fluid dynamics within manifold and SCD burner. Novel digital signal processing and phase-locked amplification of the detector signal enhances the precision and temporal resolution of the CSD. What this means is that the CSD is capable of measuring low level sulfur dioxide (< 20 pptv) in less than one minute. The high temporal resolution and sensitivity of the CSD allows for more detailed study of the atmosphere form a moving platform such as an airplane. The DD/SCD and CSD have applications in many fields where sulfur dioxide is found in air, including process stream monitoring, pollution source monitoring and pollution receptor/compliance monitoring as required by the Clean Air Act.

Development and evaluation of an automated, high precision calibration system for gaseous samples.
A source of precise, accurate and reproducible calibration gas is crucial for making meaningful measurements of trace gases in the atmosphere. We have developed an automated calibration system that can quickly deliver test gases from pptv levels to part-per-million by volume (ppmv). The system is designed so that the calibration gases delivered from the calibration system only come in contact with inert, perfluoroalkoxy (PFA) Teflon. This feature was especially important for delivering low mixing ratios of SO2 for the NSF sponsored test mentioned above, as SO2 can readily stick to other surfaces. A TCP/IP based communications interface is currently being developed for the dilution system. This interface would be an ideal calibration solution for instruments deployed in remote areas.